TiSi2 is Titanium Disilicide structured and crystallizes in the orthorhombic Fddd space group. The structure is three-dimensional. Ti is bonded in a 10-coordinate geometry to ten equivalent Si atoms. There are a spread of Ti–Si bond distances ranging from 2.56–2.78 Å. Si is bonded in a 10-coordinate geometry to five equivalent Ti and five equivalent Si atoms. There are a spread of Si–Si bond distances ranging from 2.54–2.80 Å.
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