Analysis of solution-phase macromolecular materials by diffusion NMR

EG Eden
Molecules such as covalent cages can adopt several shapes, in which the ratio of starting materials is the same, but the number of starting materials, and the shape of the resulting molecule is different. However, determining this in the absence of a crystal structure can be challenging. Pulsed field gradient (PFG) NMR has been used for two decades to characterise large macromolecules in solution, but it is still difficult to determine precise structural information, because...
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