Identification of a synthetic cannabinoid 5F-NPB-22 (indazole analog 5F-PB-22) by gas chromatography/mass spectrometry (GC/MS) method

Robert Bachliński & Agnieszka Mroczek
This article presents the problem of transesterification of a synthetic cannabinoid 5F-NPB-22 and other structurally related indazole and indole-based compounds, such as NPB-22, 5F-PB-22, BB-22 and PB-22, caused by methanol – a solvent commonly applied in gas chromatography/mass spectrometry (GC/MS) analysis. The above process can result in drawing incorrect conclusions about the composition of analyzed product, due to the formation of ester compounds, which mainly affects the reliability of results. In the present study, in...
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