The overall objective of this study was to develop cost-effective treatment processes for 1,4-dioxane removal that were safe and easy to scale up. Degradation of 1,4-dioxane was conducted and compared for the first time by heterogeneous photocatalysis and a photo-Fenton-like process under cool white fluorescent light in mild conditions, using two types of commercial nanoparticles―titanium dioxide (TiO2) and nanoscale zero-valent iron (nZVI), respectively. Both types of nanoparticles removed >99.9% of 1,4-dioxane in a short period...